Macroscale & Microscale Organic Experiments by Kenneth L. Williamson

Description: About this productProduct InformationThe market leader for the full-year organic laboratory, this manual derives many experiments and procedures from the classic Feiser lab text, giving it an unsurpassed reputation for solid, authoritative content. The Williamson/Minard/Masters manual's flexible mix of macroscale and microscale options for most experiments allows instructors to save on the purchase and disposal of expensive, sometimes hazardous organic chemicals. Macroscale versions can be used for less costly experiments, giving students experience working with conventionally sized glassware. The Fifth Edition of the manual includes new experiments that stress greener chemistry, revised content in computational chemistry, and more information on laboratory safety procedures.Product IdentifiersPublisherCengage LearningISBN-100618590676ISBN-139780618590674eBay Product ID (ePID)52888349Product Key FeaturesAuthorRobert Minard, Kenneth Williamson, Katherine M. MastersPublication NameMacroscale and Microscale Organic ExperimentsFormatHardcoverLanguageEnglishPublication Year2006TypeTextbookNumber of Pages880 PagesDimensionsItem Length9.4in.Item Height1.4in.Item Width7.7in.Item Weight52.6 OzAdditional Product FeaturesLc Classification NumberQd261.W54 2007Edition Number5Table of ContentPreliminary Contents I. Introduction 1. Introduction 2. Laboratory Safety, Courtesy, and Waste Disposal II. Techniques 3. Melting Points and Boiling Points 4. Recrystallization 5. Distillation 6. Steam Distillation, Vacuum Distillation, and Sublimation 7. Extraction 8. Thin-Layer Chromatography: Analysis of Analgesics and Isolation of Lycopene from Tomato Paste 9. Column Chromatography: Fluorenone, Acetylferrocene, Cholesteryl Acetate, and Plant Pigments 10. Gas Chromatography: Analysis of Alkene Isomers 11. Infrared Spectroscopy 12. Nuclear Magnetic Resonance Spectroscopy 13. Mass Spectroscopy 14. Ultraviolet Spectroscopy, Refractive Indices, and Qualitative Instrumental Organic Chemistry 15. Computational Chemistry III. Elimination, Substitution, and Addition 16. The SN2 Reaction: 1-Bromobutane 17. Nucleophilic Substitution Reactions of Alkyl Halides 18. Radical Initiated Chlorination of 1-Chlorobutane 19. Alkenes from Alcohols: Cyclohexene from Cyclohexanol 20. Bromination and Debromination: Purification of Cholesterol 21. Dichlorocarbene IV. Oxidation and Reduction 22. Oxidation: Cyclohexanol to Cyclohexanone; Cyclohexanone to Adipic Acid 23. Pulegone from Citronellol: Oxidation with Pyridinium Chlorochromate 24. Oxidative Coupling of Alkynes: 2,7-Dimethyl-3,5-octadiyn-2,7-diol 25. Catalytic Hydrogenation 26. Borohydride Reduction of 2-Methylcyclohexanone: A Problem in Conformational Analysis 27. Epoxidation of Cholesterol V. Aromatic Substitution and Elimination 28. Nitration of Methyl Benzoate 29. Friedel-Crafts Alkylation of Benzene and Dimethoxybenzene; Host-Guest Chemistry 30. Alkylation of Mesitylene 31. Reactions of Triphenylmethyl Carbocation, Carbanion, and Radical 32. The Friedel-Crafts Reaction: Anthraquinone and Anthracene 33. Friedel-Crafts Acylation of Ferrocene: Acetylferrocene 34. 1,2,3,4-Tetraphenylnaphthalene via Benzyne 35. Triptycene via Benzyne VI. Reactions of Aldehydes and Ketones 36. Aldehydes and Ketones 37. Dibenzalacetone by the Aldol Condensation 38. Grignard Synthesis of Triphenylmethanol and Benzoic Acid 39. The Wittig and Wittig-Horner Reactions VII. Reactions of Carboxylic Acids, Esters, and Amines 40. Esterification and Hydrolysis 41. Acetylsalicylic Acid (Aspirin) 42. Malonic Ester of a Barbiturate 43. Amines VIII. Derivatives of 1,2-Diphenylethane: A Multistep Process 44. The Sandmeyer Reaction: 1-Bromo-4-chlorobenzene, 2-Iodobenzoic Acid, and 4-Chlorotoluene 45. Sulfanilamide from Nitrobenzene 46. Dyes and Dyeing 47. Martius Yellow IX. The Diels-Alder and Related Reactions 48. Diels-Alder Reaction 49. Ferrocene [Bis(cyclopentadienyl)iron] 50. p-Terphenyl by the Diels-Alder Reaction 51. Tetraphenylcyclopentadienone 52. Hexaphenylbenzene and Dimethyl Tetraphenylphthalate X. Derivatives of 1,2-Diphenylethane: A Multistep Synthesis 53. The Benzoin Condensation: Cyanide Ion and Thiamine Catalyzed 54. Nitric Acid Oxidation. Preparation of Benzil from Benzoin. Synthesis of a Heterocycle: Diphenylquinoxaline 55. Borohydride Reduction of a Ketone: Hydrobenzoin from Benzil 56. Synthesis of 2,2-Dimethyl-1,5-dioxolane. The Acetonide Derivative of a Vicinal Diol 57. 1,4-Addition: Reductive Acetylation of Benzil 58. Synthesis of an Alkyne from an Alkene. Bromination and Dehydrobromination: Stilbene and Diphenylacetylene 59. The Perkin Reaction: Synthesis of -Phenylcinnamic Acid 60. Decarboxylation: Synthesis of cis-Stilbene XI. Photochemistry 61. Chemiluminescence: Syntheses of Cyalume and Luminol 62. Photochemistry: The Synthesis of Benzopinacol XII. Natural Product Chemistry and Biochemistry 63. Carbohydrates and Sweeteners 64. Biosynthesis of Ethanol 65. Enzymatic Reactions: A Chiral Alcohol from a Ketone and Enzymatic Resolution of dl-Alanine 66. The Synthesis of Natural Products: Pseudopellitierene and Camphor 67. Polymers: Synthesis and Recycling XIII. Searching the Chemical Literature 68. Searching the Chemical LiteratureCopyright Date2007Target AudienceCollege AudienceTopicGeneral, Chemistry / OrganicLccn2005-930127Dewey Decimal547.0078Dewey Edition23IllustratedYesGenreEducation, Science

Price: 13.98 USD

Location: Multiple Locations

End Time: 2024-05-08T22:57:21.000Z

Shipping Cost: 3.97 USD